HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Aminoethyl)piperidine, 4-BOC protected → HCID 66821595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Aminoethyl)piperidine, 4-BOC protected | HCID 1501849 | — |
| Reactant | HCID 66818709 | HCID 66818709 | — |
| Product | HCID 66821595 | HCID 66821595 | 66.5% |
Reaction Steps
6-(4-Cyano phenoxy)-2-(4-trifluoromethoxy phenoxy)nicotinic acid (0.15 g, 0.36 mmol) and (2-piperidin-4-yl-ethyl)-carbamic acid tert-butyl ester (0.082 g, 0.36 mmol) were coupled using the procedure of Example 5(c) to afford 0.15 g of the required product. Percentage purity (LCMS): 43.23%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-8da125c9e84746bca19bbb936334b60f |
| Source note | uspto-grants-2014_05 |