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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1024725Generated: November 1, 2026

Diethylamine → HCID 66818676, compound

https://huagongshe.com/reaction/1024725

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantHCID 66818818HCID 66818818—
ProductHCID 66818676HCID 6681867672.3%

Reaction Steps

Following the procedure of Example 5(c) 3,5-bis-(4-cyano-phenoxy)-benzoic acid 1.2 g (3.36 mmol) and diethyl-amine (0.245 g, 3.36 mmol) were used to afford 1.0 g of the required product. 1H NMR (DMSO-d6): δ 1.15 (6H, m), 3.22 (2H, m), 3.40 (2H, m), 6.94 (2H, d), 7.05 (1H, t), 7.25 (2H, d), 7.88 (2H, d).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722930B2
Source datasetuspto-grants-2014_05
ORD IDord-4abe7342802d478c94f8e80dd43da264
Source noteuspto-grants-2014_05