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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1024764Generated: October 30, 2026

Benzoic acid, 3,5-dihydroxy-, ethyl ester → HCID 67608049, compound

https://huagongshe.com/reaction/1024764

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoic acid, 3,5-dihydroxy-, ethyl esterHCID 20098—
ReactantBenzonitrile, 3-(bromomethyl)-HCID 97249—
ProductHCID 67608049HCID 6760804975.3%

Reaction Steps

3,5-Dihydroxy benzoic acid ethyl ester (1.45 g, 7.95 mmol) and 3-bromomethyl-benzonitrile (6.23 g, 31.8 mmol) and other reagents as described in Example 75(a) were used to afford 2.3 g of the required product. 1H NMR (DMSO-d6): 1.15 (3H, t), 4.15 (2H, q), 5.3 (4H, s), 7.0 (1H, s), 7.18 (2H, s), 7.64 (4H, d), 7.86 (4H, d).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08722930B2
Source datasetuspto-grants-2014_05
ORD IDord-0c145b30d3e14c45a1dea9354e9ce79d
Source noteuspto-grants-2014_05