HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 3,5-dihydroxy-, ethyl ester → HCID 67608049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 3,5-dihydroxy-, ethyl ester | HCID 20098 | — |
| Reactant | Benzonitrile, 3-(bromomethyl)- | HCID 97249 | — |
| Product | HCID 67608049 | HCID 67608049 | 75.3% |
Reaction Steps
3,5-Dihydroxy benzoic acid ethyl ester (1.45 g, 7.95 mmol) and 3-bromomethyl-benzonitrile (6.23 g, 31.8 mmol) and other reagents as described in Example 75(a) were used to afford 2.3 g of the required product. 1H NMR (DMSO-d6): 1.15 (3H, t), 4.15 (2H, q), 5.3 (4H, s), 7.0 (1H, s), 7.18 (2H, s), 7.64 (4H, d), 7.86 (4H, d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-0c145b30d3e14c45a1dea9354e9ce79d |
| Source note | uspto-grants-2014_05 |