Acetic Anhydride → HCID 86665959, compound

Participants

Reaction Steps

{4-[3-[4-(N-Hydroxycarbamimidoyl)phenoxy]-5-(octahydroquinoline-1-carbonyl)-phenoxyl]benzyl}carbamic acid tert-butyl ester, 1.4 g (2.28 mmol) was acetylated with 0.26 g (2.5 mmol) of acetic anhydride using the procedure of Example 2(e) to afford 1.04 g of the required product. Percentage purity (LCMS): 36.1%, (M+1)=654.3+1.

Provenance & Evidence