HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → HCID 66818769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | HCID 66818786 | HCID 66818786 | — |
| Product | HCID 66818769 | HCID 66818769 | 72.7% |
Reaction Steps
Following procedure of Example 11(e) 3,5-bis-(4-cyano-phenoxy)-N-piperidin-4-yl-benzamide 0.5 g (1.14 mmol) and 2-bromoethanol (0.214 g, 1.71 mmol) were used to afford 0.4 g of the required product. Percentage purity (LCMS): 76.2%, (M+1)=482+1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08722930B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-81cfea82adbf43569d2dfb8813017baf |
| Source note | uspto-grants-2014_05 |