HRID1024896

反应详情

EQUATION

反应方程式

HRID 1024896 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from 1-methyl-1H-imidazole-4-sulfonamide (0.19 g) and 4-Chloro-2-[[(2,3-difluorophenyl)methyl]thio]-6-methoxypyrimidine (the product of Example 35, step i) (0.25 g) according to the procedure outlined in Example 1, step iv). The crude material was purified by column chromatography using EtOAc/isohexane (2:8) as eluent. Yield: 0.11 g.

WORKUP

后处理

  1. customThe crude material was purified by column chromatography