HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(azepan-1-yl)-N-benzyl-N-methylpropan-1-amine → 3-(Azepan-1-yl)-N-methylpropan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(azepan-1-yl)-N-benzyl-N-methylpropan-1-amine | HCID 58540516 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(Azepan-1-yl)-N-methylpropan-1-amine | HCID 20600700 | — |
Reaction Steps
3-(Azepan-1-yl)-N-benzyl-N-methylpropan-1-amine (100 mg) was dissolved in MeOH (20 mL) and to the solution was added 10% Pd/C (50 mg). The reaction mixture was shook under 50 psi hydrogen atmosphere for 2 h. The catalyst was filtered over Cellite and washed with methanol. The filtrated was evaporated to give 3-(azepan-1-yl)-N-methylpropan-1-amine, used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729081B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-0cee089173a14ebd94458429875714a0 |
| Source note | uspto-grants-2014_05 |