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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1025418Generated: November 1, 2026

Isopropylamine → HCID 68207821, compound

https://huagongshe.com/reaction/1025418

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsopropylamineHCID 6363—
ReactantMethyl 3-(bromomethyl)benzoateHCID 517981—
SolventDimethylformamideHCID 6228—
ProductHCID 68207821HCID 6820782166.3%

Reaction Steps

A mixture of 2.00 g of methyl 3-(bromomethyl)benzoate, 1.55 g of isopropylamine, and 10 mL of DMF was stirred at room temperature overnight. The reaction mixture was concentrated under reduced pressure and the obtained residue was purified by silica gel column chromatography (chloroform-methanol) to obtain 1.20 g of methyl 3-[(isopropylamino)methyl]benzoate as a colorless solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08729068B2
Source datasetuspto-grants-2014_05
ORD IDord-0a86009b9b98468abb83647f7c1ae0d7
Source noteuspto-grants-2014_05