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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1026255Generated: October 31, 2026

Triethyl phosphite → HCID 67777907, compound

https://huagongshe.com/reaction/1026255

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethyl phosphiteHCID 31215—
ReactantHCID 136372363HCID 136372363—
ProductHCID 67777907HCID 67777907—

Reaction Conditions

Temperature140 °C

Reaction Steps

A mixture of 4-{[4-(cyclopropylmethoxy)-2-nitrophenyl]diazenyl}phenol and triethyl phosphite (4 mL) was stirred at 140° C. overnight. The reaction mixture was purified by silica gel column chromatography (hexane/ethyl acetate) to give the title compound as a yellow solid (103 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08729102B2
Source datasetuspto-grants-2014_05
ORD IDord-705e89c5c32d4f2f9201dbe36ceaa156
Source noteuspto-grants-2014_05