HRID1026669

反应详情

EQUATION

反应方程式

HRID 1026669 的结构方程式

PROCEDURE

实验过程

The title compound was prepared by reacting (S)—N-{3-[4-(4-oxo-piperidin-1-yl)-3-fluorophenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (1.2 mmol) with methylmagnecium bromide (1.32 mmol) in tetrahydrofuran (20 ml) at a temperature 0° C. to 25° C. for twelve hours and by purifying the compound by silica gel column chromatography in 71% yield.

WORKUP

后处理

  1. customat a temperature 0° C. to 25° C.
  2. customfor twelve hours
  3. customby purifying the compound by silica gel column chromatography in 71% yield