HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 60133465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 59754123 | HCID 59754123 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 60133465 | HCID 60133465 | 85% |
Reaction Steps
The title compound was prepared by reacting (S)—N-{3-[4-(4-oxo-piperidin-1-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide (1.0 mmol), with sodiumborohydride (1.2 mmol)) methanol (10 ml) at a temperature 0-25° C. for 2 hours in 85% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729269B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-33be73423ca24eba8e0dcd5bcddbc651 |
| Source note | uspto-grants-2014_05 |