Methyl iodide → HCID 67134619, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 820 mg (3.3 mmol) of 1,4-dibutyl-2-methyl-1,4,2-diazaphospholidine-3,5-dione (cf. Ex. 3) with 6.27 g (44 mmol) of methyl iodide (from Aldrich) was heated at reflux (bath temperature: to 80° C.) while stirring with a magnetic stirrer bar for 24 h. The yellow mixture, whose viscosity had risen noticeably, was analysed by NMR spectroscopy without further workup:

Provenance & Evidence