HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methylaniline → HCID 67539989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methylaniline | HCID 262970 | — |
| Reactant | 7-Chloro-3-ethoxycarbonyl-6-[4-(4-fluorophenyl)piperidine-1-carbonyl]pyrazolo[1,5-a]pyrimidine | HCID 86646293 | — |
| Product | HCID 67539989 | HCID 67539989 | 99.9% |
Reaction Steps
In the same manner as in Example 19, step 5 and using 7-chloro-3-ethoxycarbonyl-6-[4-(4-fluorophenyl)piperidine-1-carbonyl]pyrazolo[1,5-a]pyrimidine (0.090 g, 0.21 mmol) obtained in step 2 and 2-fluoro-5-methylaniline (0.053 g, 0.42 mmol), the title compound (0.109 g, 99%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729264B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-957d7f7c02814f1795e9f891657916c8 |
| Source note | uspto-grants-2014_05 |