HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethylaniline → HCID 67541263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethylaniline | HCID 7259 | — |
| Reactant | Ethyl 3-bromo-7-chloropyrazolo[1,5-a]pyrimidine-6-carboxylate | HCID 57345881 | — |
| Product | HCID 67541263 | HCID 67541263 | 68% |
Reaction Steps
In the same manner as in Example 1, step 4 and using ethyl 3-bromo-7-chloropyrazolo[1,5-a]pyrimidine-6-carboxylate (400 mg, 1.31 mmol) obtained in Example 22, step 1 and 2,5-dimethylaniline (0.19 mL, 1.57 mmol), the title compound (345 mg, 68%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729264B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-f57b2c51a69b4800a36f3ba8ef97cb23 |
| Source note | uspto-grants-2014_05 |