HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylspiro[inden-1,4'-piperidine] → HCID 178469962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylspiro[inden-1,4'-piperidine] | HCID 67540763 | — |
| Reactant | HCID 178469973 | HCID 178469973 | — |
| Product | HCID 178469962 | HCID 178469962 | 77.7% |
Reaction Steps
In the same manner as in Example 19, step 3 and using 3-ethoxycarbonyl-7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylic acid (0.533 g, 2.12 mmol) obtained in Example 19, step 2 and 2-methylspiro[inden-1,4′-piperidine] (0.465 g, 2.34 mmol), the title compound (0.712 g, 70%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729264B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-ee1a6cbbee8647fa9296063b1e7be346 |
| Source note | uspto-grants-2014_05 |