HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methylaniline → HCID 67541230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methylaniline | HCID 262970 | — |
| Reactant | HCID 86646299 | HCID 86646299 | — |
| Product | HCID 67541230 | HCID 67541230 | 52% |
Reaction Steps
In the same manner as in Example 19, step 5 and using 7-chloro-3-ethoxycarbonyl-6-(7-fluoro-2H-spiro[benzofuran-3,4′-piperidine]-1′-ylcarbonyl)pyrazolo[1,5-a]pyrimidine (0.250 g, 0.546 mmol) obtained in Example 145, step 2 and 2-fluoro-5-methylphenylamine (0.150 mL, 1.37 mmol), the title compound (0.155 g, 52%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08729264B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-df680001fb294f6eadc508a165146a96 |
| Source note | uspto-grants-2014_05 |