HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178503523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 178503566 | HCID 178503566 | — |
| Solvent | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 178503523 | HCID 178503523 | 38.6% |
Reaction Steps
21 g of N-(4,6-dihydroxy-2-methylsulfanyl-pyrimidin-5-yl)-3-methyl-benzamide in 100 ml of phosphorus oxychloride were heated to 70° C. for 3 h. After cooling, the mixture was poured into 500 ml of diethyl ether. The precipitate was filtered off and washed with diethyl ether. 7.6 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735387B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-7623b55efad844c793a76286241d0ccb |
| Source note | uspto-grants-2014_05 |