HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dipropyl disulfide → HCID 178460778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dipropyl disulfide | HCID 12377 | — |
| Reactant | HCID 178419464 | HCID 178419464 | — |
| Reactant | HCID 178503312 | HCID 178503312 | — |
| Solvent | Diethylether ethylacetate | HCID 21584169 | — |
| Product | HCID 178460778 | HCID 178460778 | 76% |
Reaction Steps
Compound 21E was prepared following the procedure as described for the synthesis of compound 21A using (see scheme 3) 1-propyldisulfanyl-propane as the disulfide and 3-(4-bromo-1H-pyrazol-3-yl)-pyridine (compound 20A). (flash chromatography conditions ethyl acetate/diethyl ether 5/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735388B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-8f4acae8420f46a7afa9ac9f8a8c86b4 |
| Source note | uspto-grants-2014_05 |