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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1027584Generated: October 31, 2026

Trifluoroacetic acid → HCID 67246433, compound

https://huagongshe.com/reaction/1027584

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 15384455HCID 15384455—
SolventDichloromethaneHCID 6344—
ProductHCID 67246433HCID 67246433—

Reaction Steps

A solution of (2-benzyl-isoxazolidin-5-ylmethyl)-carbamic acid tert-butyl ester (Step A, 0.5 g) in dichloromethane (10 ml) was treated with trifluoroacetic acid (1.95 g). The solution was stirred at room temperature for 4 hours then concentrated in vacuo to afford the crude title product, which was used directly for the next step. LCMS (Method F) 0.20 min, M+H 194.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08735362B2
Source datasetuspto-grants-2014_05
ORD IDord-898f86f6e4c34faf8f288b5596f240ef
Source noteuspto-grants-2014_05