L-Phenylalanine → HCID 59193234, compound

HRID 1027778Notes

Reaction equation

HRID 1027778 reaction equation
[C:1]([NH:24][CH:25]([CH2:39][CH:40]([CH3:42])[CH3:41])[C:26]([NH:28][C:29]1[CH:30]=[CH:31][C:32]([OH:38])=[C:33]([CH:37]=1)[C:34]([OH:36])=[O:35])=[O:27])(=[O:23])[CH2:2][CH2:3]/[CH:4]=[CH:5]\[CH2:6]/[CH:7]=[CH:8]\[CH2:9]/[CH:10]=[CH:11]\[CH2:12]/[CH:13]=[CH:14]\[CH2:15]/[CH:16]=[CH:17]\[CH2:18]/[CH:19]=[CH:20]\[CH2:21][CH3:22].N[C@H:44]([C:52](O)=O)[CH2:45]C1C=CC=CC=1>>[C:1]([NH:24][CH:25]([CH2:39][C:40]1[CH:41]=[CH:52][CH:44]=[CH:45][CH:42]=1)[C:26]([NH:28][C:29]1[CH:30]=[CH:31][C:32]([OH:38])=[C:33]([CH:37]=1)[C:34]([OH:36])=[O:35])=[O:27])(=[O:23])[CH2:2][CH2:3]/[CH:4]=[CH:5]\[CH2:6]/[CH:7]=[CH:8]\[CH2:9]/[CH:10]=[CH:11]\[CH2:12]/[CH:13]=[CH:14]\[CH2:15]/[CH:16]=[CH:17]\[CH2:18]/[CH:19]=[CH:20]\[CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 6140L-PhenylalanineHCID 446260545-(2-(4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4, 7,10,13,16,19-hexaenamido-4-methylpentanamido)-2-hydroxybenzoic acid

Product 1

HCID 59193234HCID 59193234, compound

Procedure

5-(2-(4Z,7Z,10Z,13Z,16Z,19Z)-Docosa-4,7,10,13,16,19-hexaenamido-3-phenylpropanamido)-2-hydroxybenzoic acid was prepared in a similar fashion as 5-(2-(4Z,7Z,10Z,13Z,16Z,19Z)-docosa-4,7,10,13,16,19-hexaenamido-4-methylpentanamido)-2-hydroxybenzoic acid, using the appropriate phenylalanine starting material. Mass calculated for C38H46N2O5=610.78. found: [M−H]+=609.3:

Sources & evidence

ORD record
ord-05af27ec83fc41eea4732cf6197126e4
Source dataset
uspto-grants-2014_05
Patent number
US08735378B2

Reaction notes

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