HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68007300, compound → HCID 68006986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68007300 | HCID 68007300 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68006986 | HCID 68006986 | — |
Reaction Steps
To a solution of 2-(3-benzyloxyphenyl)-9-methyl-7-(pyrrolidin-1-ylcarbonyl)-7,9-dihydro-8H-purine-8-one <the compound of Example 202> (30 mg) in methanol (10 ml) was added 10% palladium on carbon (3 mg) and the mixture was stirred for 4 hours at room temperature under hydrogen atmosphere. After removing the catalyst from the reaction mixture, the solvent was evaporated under reduced pressure, and the residue was dried to give the title compound 24 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735406B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-c1f3ecae744140babbc8fac1f1e360f5 |
| Source note | uspto-grants-2014_05 |