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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1027793Generated: October 30, 2026

HCID 68007300, compound → HCID 68006986, compound

https://huagongshe.com/reaction/1027793

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68007300HCID 68007300—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 68006986HCID 68006986—

Reaction Steps

To a solution of 2-(3-benzyloxyphenyl)-9-methyl-7-(pyrrolidin-1-ylcarbonyl)-7,9-dihydro-8H-purine-8-one <the compound of Example 202> (30 mg) in methanol (10 ml) was added 10% palladium on carbon (3 mg) and the mixture was stirred for 4 hours at room temperature under hydrogen atmosphere. After removing the catalyst from the reaction mixture, the solvent was evaporated under reduced pressure, and the residue was dried to give the title compound 24 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08735406B2
Source datasetuspto-grants-2014_05
ORD IDord-c1f3ecae744140babbc8fac1f1e360f5
Source noteuspto-grants-2014_05