HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68006945, compound → HCID 68007030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68006945 | HCID 68006945 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68007030 | HCID 68007030 | — |
Reaction Steps
To a solution of 2-(3-nitrophenyl)-9-methyl-7-(pyrrolidin-1-ylcarbonyl)-7,9-dihydro-8H-purine-8-one <the compound of Example 203> (41 mg) in methanol (10 ml) was added 10% palladium on carbon (10 mg) and the mixture was stirred for 2 hours at room temperature under hydrogen atmosphere. After removing the catalyst from the reaction mixture, the solvent was evaporated under reduced pressure, and the residue was dried to give the title compound 35 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735406B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-4d2f5141dc1341a085ca79ac56e314ce |
| Source note | uspto-grants-2014_05 |