HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59637336, compound → HCID 59637291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59637336 | HCID 59637336 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59637291 | HCID 59637291 | — |
Reaction Steps
Ethyl 2-cyclohexyl-2-(3-fluoro-4-nitrophenyl)acetate was dissolved in a 1:1 mixture of EtOH and EA (420 mL) and hydrogenation was carried out in an H-cube (1 bar, 25° C., 1 mL/min and 0.25 mol/L). Following removal of the solvent and drying, 5 g of the desired product were obtained (quantitative conversion).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735426B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-7e7d883b4f43452d9961155ec486cbf3 |
| Source note | uspto-grants-2014_05 |