HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59637316, compound → HCID 59637311, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59637316 | HCID 59637316 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59637311 | HCID 59637311 | 97.5% |
Reaction Steps
Ethyl 2-phenyl-2-(3-fluoro-4-nitrophenyl)acetate was dissolved in a 1:1 mixture of EtOH and EA (465 mL) and hydrogenation was carried out in an H-cube (1 bar, 25° C., 1 mL/min and 0.25 mol/L). Following removal of the solvent and drying, 5.2 g (97.5%) of product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735426B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-504da8a34350489fa7b90d17a3d30252 |
| Source note | uspto-grants-2014_05 |