HRID1028266

反应详情

EQUATION

反应方程式

HRID 1028266 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

36 g of styrene (ST), 4 g of N-phenylmaleimide (PM), 100 mg of azobisisobutyronitrile, and 50 ml of toluene were mixed, and a polymerization reaction was performed under a nitrogen atmosphere at 85° C. for 6 hours. After cooling, purification was performed by reprecipitation using chloroform-hexane. Thus, 25.6 g of an ST-PM (90:10) random copolymer (Mn=43000) was obtained.

WORKUP

后处理

  1. customa polymerization reaction
  2. temperatureAfter cooling
  3. custompurification
  4. customwas performed by reprecipitation