HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetanilide → HCID 25216870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetanilide | HCID 904 | — |
| Reactant | 2-Bromo-4-fluoro-1-nitrobenzene | HCID 2756993 | — |
| Product | HCID 25216870 | HCID 25216870 | 66% |
Reaction Steps
The title compound was prepared with the analogous procedure described in example 3 using 1-Bromo-5-fluoro-2-nitrobenzene and N-phenylacetamide (81 mg, 0.6 mmol) as starting materials to yield the title compound as brown solid (75 mg, 66%). 1H NMR (DMSO) δ 2.50 (s, 3 H), 7.11 (d, 1 H), 7.21-7.29 (m, 1H), 7.59-7.69 (m, 5 H), 7.79 (br s, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735586B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-43645468bd1448648ad18c8631b90f43 |
| Source note | uspto-grants-2014_05 |