HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 1319196-91-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1319196-91-2 | HCID 67324218 | — |
Reaction Steps
To a solution of 4-fluoro-2-methylaniline (5.0 g, 40.0 mmol) in DCM (100 mL) at RT was added bromine (2.06 mL, 40.0 mmol). The reagent appeared to react instantly and a solid precipitate was formed. The reaction was filtered and washed with DCM to give 2-bromo-4-fluoro-6-methylaniline hydrobromide as a light tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735384B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-c8a10f06837c4d66a99954dad1018f3e |
| Source note | uspto-grants-2014_05 |