HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Chlorophenyl)boronic acid → HCID 58168319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Chlorophenyl)boronic acid | HCID 2734323 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168319 | HCID 58168319 | 14% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 153 using Compound 83 (50 mg, 0.22 mmol) and 3-chloro-phenylboronic acid (44 mg, 0.33 mmol) to provide 155 (9 mg, 14% yield) as a white solid. LC-MS (M+H=307, obsd.=307).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-1e596e3030c54705b91d6a722163d3b2 |
| Source note | uspto-grants-2014_05 |