HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-methoxybenzonitrile → HCID 58168273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-methoxybenzonitrile | HCID 12715714 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168273 | HCID 58168273 | 87% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 113 using Compound 83 (100 mg, 0.43 mmol) and 2-amino-6-methoxy-benzonitrile (77 mg, 0.52 mmol) to provide 157 (128 mg, 86% yield) as a yellow solid. LC-MS (M+H=343, obsd.=343).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-e7c95535772a4e9ebc3d2ac4c35ec8f5 |
| Source note | uspto-grants-2014_05 |