HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1029143Generated: November 2, 2026
HCID 58168295, compound → HCID 69815544, compound
https://huagongshe.com/reaction/1029143
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 58168295 | HCID 58168295 | — |
| Solvent | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 69815544 | HCID 69815544 | 118.9% |
Reaction Steps
Compound 178 (70 mg, 0.18 mmol) was dissolved in 1.5 M HCl/MeOH (5 mL), and stirred for 4 h at 60° C. The reaction solution was concentrated, and the resulting precipitate was dried under vacuum to provide 179 (60 mg, 92% yield) as a white solid. LC-MS (M+H=281, obsd.=281).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08735584B2 |
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| Source dataset | uspto-grants-2014_05 |
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| ORD ID | ord-2fcb9fd399304be9b000cde9afbf5e1a |
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| Source note | uspto-grants-2014_05 |
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