HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxyaniline → HCID 58168212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxyaniline | HCID 7613 | — |
| Reactant | 1-Chlorobenzo[C][1,8]naphthyridin-6(5H)-one | HCID 58168008 | — |
| Product | HCID 58168212 | HCID 58168212 | 76.3% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 188 using Compound 83 (100 mg, 0.43 mmol) and 2,5-di-methoxyaniline (133 mg, 0.87 mmol) to provide 200 (114 mg, 76% yield) as a white solid. LC-MS (M+H=348, obsd.=348).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-d5cd69fa26cb4d7cb406d5e242caeec4 |
| Source note | uspto-grants-2014_05 |