HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-iodopyridin-2-amine → HCID 58168232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-iodopyridin-2-amine | HCID 22936596 | — |
| Reactant | HCID 68648691 | HCID 68648691 | — |
| Product | HCID 58168232 | HCID 58168232 | 17.2% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 1 using 4-chloro-3-iodopyridin-2-amine (500 mg, 1.96 mmol) and 2-methoxycarbonyl-4-hydroxy-phenylboronic acid (765 mg, 2.75 mmol) to provide 217 (83 mg, 17% yield) as a white solid. LC-MS (M+H=247, obsd.=247).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-e810c770b1f14f1383cdc1ee54f17254 |
| Source note | uspto-grants-2014_05 |