HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 58168190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | 9-chloro-5H-benzo[c][1,8]naphthyridin-6-one | HCID 58168298 | — |
| Product | HCID 58168190 | HCID 58168190 | 25.3% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 231 using 6 (50 mg, 0.22 mmol) and 4-fluoroaniline (0.03 mL, 0.33 mmol) to provide 235 (17 mg, 23% yield) as a green/brown solid. LC-MS (M+H=306, obsd.=306).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-11369d75c5b74313aacbf396365baa3b |
| Source note | uspto-grants-2014_05 |