HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Toluidine → HCID 58168041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Toluidine | HCID 7934 | — |
| Reactant | 9-chloro-5H-benzo[c][1,8]naphthyridin-6-one | HCID 58168298 | — |
| Product | HCID 58168041 | HCID 58168041 | 22.4% |
Reaction Steps
The title compound was synthesized according to the procedure described for the preparation of Example 231 using 6 (100 mg, 0.43 mmol) and m-toluidine (0.07 mL, 0.65 mmol) to provide 241 (29 mg, 20% yield) as a black powder. LC-MS (M+H (parent)=302, obsd.=302).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08735584B2 |
| Source dataset | uspto-grants-2014_05 |
| ORD ID | ord-0fbd2dc9ed9343f6bf6934122b15c82e |
| Source note | uspto-grants-2014_05 |