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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1029434Generated: October 31, 2026

HCID 15780326, compound → HCID 19037524, compound

https://huagongshe.com/reaction/1029434

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15780326HCID 15780326—
SolventMethanolHCID 887—
ProductHCID 19037524HCID 1903752469.3%

Reaction Steps

2-[1-(α-Chloroethylcarbamoyl)-4-piperidinyl]-5-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indol-1-one (0.300 g) was dissolved in anhydrous methanol (6 ml), and the solution was heated under reflux for 4 hrs. The reaction mixture was evaporated, and the residue was recrystallized from absolute ethanol to afford 0.10 g (50%) of product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05102889
Source datasetuspto-grants-1992_04
ORD IDord-5ccaa1a0a242495e8048d2c9197c89c0
Source noteuspto-grants-1992_04