HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15780326, compound → HCID 19037524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15780326 | HCID 15780326 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19037524 | HCID 19037524 | 69.3% |
Reaction Steps
2-[1-(α-Chloroethylcarbamoyl)-4-piperidinyl]-5-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indol-1-one (0.300 g) was dissolved in anhydrous methanol (6 ml), and the solution was heated under reflux for 4 hrs. The reaction mixture was evaporated, and the residue was recrystallized from absolute ethanol to afford 0.10 g (50%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05102889 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-5ccaa1a0a242495e8048d2c9197c89c0 |
| Source note | uspto-grants-1992_04 |