HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-Diisopropylaminopropionic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-methylpiperidine-3-carboxylic Acid | HCID 2736937 | — |
| Reactant | Ethyl 3-diisopropylaminopropionate | HCID 15468050 | — |
| Product | 3-Diisopropylaminopropionic acid hydrochloride | HCID 86745623 | — |
Reaction Steps
3-Diisopropylaminopropionic acid hydrochloride may be obtained by working according to the method described in Example 4 for the preparation of 1-methyl-3-piperidinecarboxylic acid, but starting with ethyl 3-diisopropylaminopropionate (5 g) and 6N aqueous hydrochloric acid solution (35 cc). After the product obtained has been recrystallized in acetone, 3-diisopropylaminopropionic acid hydrochloride (2.3 g), m.p. 170° C., is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05102890 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-d5b63bbaf0944c59a6cb75fd9d679952 |
| Source note | uspto-grants-1992_04 |