HRID1029479

反应详情

EQUATION

反应方程式

HRID 1029479 的结构方程式

PROCEDURE

实验过程

3-Diisopropylaminopropionic acid hydrochloride may be obtained by working according to the method described in Example 4 for the preparation of 1-methyl-3-piperidinecarboxylic acid, but starting with ethyl 3-diisopropylaminopropionate (5 g) and 6N aqueous hydrochloric acid solution (35 cc). After the product obtained has been recrystallized in acetone, 3-diisopropylaminopropionic acid hydrochloride (2.3 g), m.p. 170° C., is obtained.

WORKUP

后处理

  1. customAfter the product obtained
  2. customhas been recrystallized in acetone