HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3-(2,6-Dimethylpiperidino)propionic acid hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Methylpiperidine-3-carboxylic acid hydrochloride | HCID 12514711 | — |
| Reactant | Ethyl 3-(2,6-dimethylpiperidino)propionate hydrochloride | HCID 19900443 | — |
| Product | 3-(2,6-Dimethylpiperidino)propionic acid hydrochloride | HCID 47000750 | — |
Reaction Steps
3-(2,6-Dimethylpiperdino)propionic acid hydrochloride may be obtained by working according to the method described in Example 4 for the preparation of 1-methyl-3-piperidinecarboxylic acid hydrochloride, but starting with ethyl 3-(2,6-dimethylpiperidino)propionate hydrochloride (12.5 g) and 6N aqueous hydrochloric acid solution (35 cc). 3-(2,6-Dimethylpiperidino)propionic acid hydrochloride, m.p. 215° C., is thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05102890 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-6cc36dfa3e534811a4cf818624daac89 |
| Source note | uspto-grants-1992_04 |