HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Diaminopyridine → HCID 178441556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Diaminopyridine | HCID 5918 | — |
| Reactant | 2-butyl-1H-imidazo[4,5-b]pyridine | HCID 12467710 | — |
| Product | HCID 178441556 | HCID 178441556 | — |
Reaction Steps
The title compound was prepared according to the procedure described for the preparation of 2-butylimidazo[4,5-b]pyridine starting with 3,4-diaminopyridine. Yield: 3.69 g (92%) thick oil: 1H NMR (300 MHz, CDCl3) δ8.93 (s, 1H), 8.35 (d, 1H, J=6 Hz), 7.48 (d, 1H, J=6 Hz), 3.01 (t, 2H, J=7 Hz), 1.92-1.82 (m, 2H), 1.48-1.30 (m, 2H), 0.86 (t, 3H, J=7 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05102880 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-b505e945b5c4490986b969e6be3466da |
| Source note | uspto-grants-1992_04 |