HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 10399099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 19901120 | HCID 19901120 | — |
| Product | HCID 10399099 | HCID 10399099 | — |
Reaction Steps
A solution of isopropyl 2-(1,3-dithietan-2-ylidene)-2-(ethoxycarboxycarbonyl)acetate (10 g) in methanolic ammonia (60 ml) was stirred at room temperature for 4 hrs. The mixture was concentrated and purified with n-hexane and ethyl ether to give the titled compound as a white solid. (5.2 g, 68%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05103013 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-5ad66801fdd64f3a85a2d015dc0df679 |
| Source note | uspto-grants-1992_04 |