Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2,7-Dichloro-3,8-dimethylquinoline | HCID 17039677 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14837868 | HCID 14837868 | 96% |
Reaction Steps
A mixture of 2.26 g of 2,7-dichloro-3,8-dimethyl-quinoline, 1.1 g of the sodium salt of 1,2,4-triazole and 10 ml of dimethyl formamide is stirred at 100° C. for 25 hours. The reaction mixture is poured into 100 ml of water and the precipitated product is filtered. Thus 2.48 g of the desired compound are obtained, yield 96%. Mp.: 147°-148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05104884 |
|---|
| Source dataset | uspto-grants-1992_04 |
|---|
| ORD ID | ord-40713b55ed164b0392ab4198662a8448 |
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| Source note | uspto-grants-1992_04 |
|---|
