化工社化工社 化学情報印刷レポート · 研究参考用
Methyl fluorosulfate → 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl fluorosulfate | HCID 9870 | — |
| 反応物 | 3-(4-Methoxybenzylthio)quinuclidine | HCID 19797265 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 3-(4-Methoxybenzylthio)-1-methylquinuclidinium fluorosulfonate | HCID 19797250 | — |
反応手順
The procedure described in preparation 6-(3) was repeated, but using 756 mg of 3-(4-methoxybenzylthio) quinuclidine and 271 μl of methyl fluorosulfonate in the presence of 5 ml of methylene chloride, to afford 1.078 g of the title compound as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05104867 |
| 出典データセット | uspto-grants-1992_04 |
| ORD ID | ord-d6f53c977c6a4da88b5af247b46a3d95 |
| 出典メモ | uspto-grants-1992_04 |