Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 668793 | HCID 668793 | — |
Reaction Steps
To an ice-cooled solution of 4-methoxybenzenesulfonyl chloride (25 g) in tetrahydrofuran (25 ml) was added dimethylamine (50% solution in water, 25 ml). After addition was complete, the mixture was stirred at 50° C. for 30 minutes. The reaction mixture was concentrated to give 4-methoxy-N,N-dimethylbenzenesulfonamide (38 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05104890 |
|---|
| Source dataset | uspto-grants-1992_04 |
|---|
| ORD ID | ord-35f86d989bd9443b827f0b008c1c2224 |
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| Source note | uspto-grants-1992_04 |
|---|
