HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 10968376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 13526351 | HCID 13526351 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 10968376 | HCID 10968376 | — |
Reaction Steps
The title compound was prepared from (S)-(-)-N-1-phenylethyl-N-trimethylsilylmethylamine by reaction with n-butanol and aqueous formaldehyde following the procedure of Example 2 to give the crude acetal (85% pure) as a colourless oil (7.1 g, 80%) δC (CD2Cl2)-1.09 (SiMe3), 14.35, 20.16, 24.72, 67.38 (OBu), 19.57 (CMe), 40.30 (NCH2Si), 62.30 (CH), 84.73 (NCH2O), 127.01, 128.15, 128.51, 146.15 (Ph).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104989 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-f367c87a673c474f93a70d2c00937dd8 |
| Source note | uspto-grants-1992_04 |