Hydrogen Peroxide → HCID 15752803, compound

Participants

Reaction Steps

To a solution of crude oily 4,4'-thiobis(6-cyclohexyl-3-methylphenol) (10.5 g) in methanol (40 ml) is gradually added dropwise 30% hydrogen peroxide (6.5 g) at room temperature. The mixture is stirred for a while at the same temperature, and left standing at 50° C. for 3 hours and overnight at room temperature. The precipitated crystals are filtered off, washed with cool methanol and dried to give 4,4'-sulfinylbis(6-cyclohexyl-3-methylphenol), m.p. 151°-153° C.

Provenance & Evidence