HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibromodifluoromethane → HCID 13315035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibromodifluoromethane | HCID 6382 | — |
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13315035 | HCID 13315035 | — |
Reaction Steps
According to this reference, 1 mole of sodium salt of p-hydroxybenzo-nitrile and 1.7 moles of dibromodifluoromethane are dissolved in dimethylformamide, stirred at the room temperature for a day and distilled to obtain desired p-(bromodifluoromethoxy)-benzonitrile. However, the yield is only about 31.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05105021 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-fd20503cb35b4855bd83e92749ef7d5c |
| Source note | uspto-grants-1992_04 |