HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Cresol → HCID 12865384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Cresol | HCID 2879 | — |
| Reactant | Dibromodifluoromethane | HCID 6382 | — |
| Reactant | Propyl mercaptan | HCID 7848 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12865384 | HCID 12865384 | 21% |
Reaction Steps
According to the process, 0.1 mole of potassium salt of p-cresol is dissolved in dimethylformamide, a catalytic amount of propanethiol is added, dibromodifluoromethane is further added, and reacted at 20° to 30° C. for 4 hours to obtain p-(bromodifluoromethoxy) toluene in a 21% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05105021 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-463c2cfc6fc7475bbefaa2715d634b23 |
| Source note | uspto-grants-1992_04 |