HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19822190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | HCID 19822257 | HCID 19822257 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19822190 | HCID 19822190 | — |
Reaction Steps
Following the same procedure as described in Preparation 18, 9 g of 6-acetoxy-2-(4-aminophenoxymethyl)-2-methyl-7-(1,1,3,3-tetramethylbutyl) chroman-4-one (prepared as described in Preparation 24), 1.8 g of sodium nitrite, 10 ml of concentrated hydrochloric acid, 20 g of ethyl acrylate, 0.3 g of cuprous oxide, 100 ml of acetone and about 8 ml of water were reacted, to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104888 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-f7b392fcb3614571ac7614ce64e78f74 |
| Source note | uspto-grants-1992_04 |