HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19822237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | HCID 19822175 | HCID 19822175 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | HCID 19822237 | HCID 19822237 | — |
Reaction Steps
Following the same procedure as described in Preparation 18, 1.6 g of 6-acetoxy-2-(4-aminophenoxymethyl)-2-(3,7-dimethyloctyl)-5,7,8-trimethylchroman-4-one (prepared as described in Preparation 32), 0.28 g of sodium nitrite, 1.7 ml of concentrated hydrochloric acid, 3.3 ml of ethyl acrylate and 0.1 g of cuprous oxide were reacted, to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104888 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-d08ebcc91ded4d1c95001c0f2c66d51f |
| Source note | uspto-grants-1992_04 |