HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19822173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Reactant | HCID 54002701 | HCID 54002701 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19822173 | HCID 19822173 | — |
Reaction Steps
Following the same procedure as described in Preparation 18, 4.5 g of 6-acetoxy-2-(5-aminopyridin-2-yloxymethyl)-2,5,7,8-tetramethylchroman (prepared as described in Preparation 37), 1.1 g of sodium nitrite, 5 ml of concentrated hydrochloric acid, 10 g of ethyl acrylate, 175 mg of cuprous oxide, 40 ml of acetone and about 2.5 g of water were reacted, to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05104888 |
| Source dataset | uspto-grants-1992_04 |
| ORD ID | ord-2dbaba3cc00645a7997df07bcea824b5 |
| Source note | uspto-grants-1992_04 |